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© Research
Publication : The journal of physical chemistry. B

Thermal decomposition of commercial silicone oil to produce high yield high surface area SiC nanorods

Scientific Fields
Diseases
Organisms
Applications
Technique

Published in The journal of physical chemistry. B - 15 Jun 2006

Pol VG, Pol SV, Gedanken A, Lim SH, Zhong Z, Lin J

Link to Pubmed [PMID] – 16771390

J Phys Chem B 2006 Jun;110(23):11237-40

This article reports on the synthesis of high surface area (563m2/g) beta-SiC nanorods by thermal decomposition of commercial silicone oil at a relatively low reaction temperature (800 degrees C) in a closed Swagelok cell. High yield (75%) of SiC nanorods are obtained in this one-stage, solvent-, catalyst-, and template-free synthesis technique that runs at a relative low temperature and employs cheap single-precursor. The morphological (TEM, HR-SEM), compositional (CHNS, EDX, SAEDX]), structural (XRD, HR-TEM, and ED), thermal (TGA) characterizations and surface area analysis are carried out for the obtained SiC nanorods. The possibility of hydrogen storage in this high surface area nano-SiC rods are also tested and reported for the first time.

https://www.ncbi.nlm.nih.gov/pubmed/16771390