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© Research
Publication : Organic letters

Palladium-Catalyzed Regio- and Stereoselective Carbothiolation of Terminal Alkynes with Azolyl Sulfides

Scientific Fields
Diseases
Organisms
Applications
Technique

Published in Organic letters - 21 Mar 2016

Iwasaki M, Topolovčan N, Hu H, Nishimura Y, Gagnot G, Na nakorn R, Yuvacharaskul R, Nakajima K, Nishihara Y

Link to Pubmed [PMID] – 26998829

Org. Lett. 2016 Apr;18(7):1642-5

Palladium-catalyzed carbothiolation of terminal alkynes with azolyl sulfides affords various 2-(azolyl)alkenyl sulfides with perfect regio- and stereoselectivities. The present addition reaction proceeded through a direct cleavage of carbon-sulfur bonds in azolyl sulfides. The resulting adducts that are useful intermediates in organic synthesis are further transformed to multisubstituted olefins containing azolyl moieties.

http://www.ncbi.nlm.nih.gov/pubmed/26998829